Development of a New Electrochemical Method for Preparation of Titanium Dioxides Films from an Aqueous Solution
- PDF / 308,832 Bytes
- 6 Pages / 432 x 648 pts Page_size
- 13 Downloads / 265 Views
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××PP ZDVULQVHGLQDFHWRQHDQG
295 Downloaded from https:/www.cambridge.org/core. University of Arizona, on 07 Apr 2017 at 19:16:52, subject to the Cambridge Core terms of use, available at https:/www.cambridge.org/core/terms. https://doi.org/10.1557/adv.2017.101
3RZHU6XSSO\ ^3RWHQWLRVWDW +RNXWR 'HQNR+$%) `
7HPSHUDWXUH &RQWUROOHU
5HIHUHQFH(OHFWURGH $J$J&O :RUNLQJ(OHFWURGH 1(6$JODVVHV &RXQWHU(OHFWURGH 3W7L6KHHW +HDWHU
)LJXUH7KHVFKHPDWLFYLHZRIHOHFWURFKHPLFDOGHSRVLWLRQV\VWHP
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
Data Loading...
