Dipolar Correlation Spectroscopy Higher-Order Correlation Terms in T
Bettina Basel presents experimental conditions which allow to extract the three-spin contribution precisely from experimental multi-spin double electron-electron resonance (DEER) signals. The theory and concepts behind the used techniques, which are among
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Springer awards „BestMasters“ to the best master’s theses which have been completed at renowned universities in Germany, Austria, and Switzerland. The studies received highest marks and were recommended for publication by supervisors. They address current issues from various fields of research in natural sciences, psychology, technology, and economics. The series addresses practitioners as well as scientists and, in particular, offers guidance for early stage researchers.
Bettina Basel
Dipolar Correlation Spectroscopy Higher-Order Correlation Terms in Three-Spin Double ElectronElectron Resonance (DEER)
Bettina Basel Erlangen, Germany
BestMasters ISBN 978-3-658-09190-3 ISBN 978-3-658-09191-0 (eBook) DOI 10.1007/978-3-658-09191-0 Library of Congress Control Number: 2015932771 Springer Spektrum © Springer Fachmedien Wiesbaden 2015 This work is subject to copyright. All rights are reserved by the Publisher, whether the whole or part of the material is concerned, specifi cally the rights of translation, reprinting, reuse of illustrations, recitation, broadcasting, reproduction on microfilms or in any other physical way, and transmission or information storage and retrieval, electronic adaptation, computer software, or by similar or dissimilar methodology now known or hereafter developed. The use of general descriptive names, registered names, trademarks, service marks, etc. in this publication does not imply, even in the absence of a specific statement, that such names are exempt from the relevant protective laws and regulations and therefore free for general use. The publisher, the authors and the editors are safe to assume that the advice and information in this book are believed to be true and accurate at the date of publication. Neither the publisher nor the authors or the editors give a warranty, express or implied, with respect to the material contained herein or for any errors or omissions that may have been made. Printed on acid-free paper Springer Spektrum is a brand of Springer Fachmedien Wiesbaden Springer Fachmedien Wiesbaden is part of Springer Science+Business Media (www.springer.com)
This book is dedicated to my chemistry teacher Markus Eiber without whom I would not have ended up in the field of chemistry after all.
Acknowledgment First of all, I would like to thank Prof. Gunnar Jeschke for giving me the chance to do my master thesis in his group and being a great boss. He always took the time for discussions and gave friendly and considered advice on how I should proceed. Moreover, I am indebted to Andrin Doll for his continuous help, for all the explanations and extra lessons he gave me and the patience he had with me. Furthermore, I am much obliged to Prof. Dirk Guldi for establishing the contact to ETH, supporting me in many aspects during all my studies and his pleasant advice. This thesis would have not been possible without the model compounds. Therefore I thank Patrick Wilhelm, Ludmila Ziegler and Prof. Helma Wennemers for synthesizing the poly(proline), Luca Garbuio for preparing the p
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