Carbonylation Direct Synthesis of Carbonyl Compounds
Since the publication of our earlier book on transition metal mediated organic synthesis, * there has been a widespread increase of interest in this topic, and transition metal based methodology has become firmly established in many areas of organic chemi
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Carbonylation Direct Synthesis of Carbonyl Compounds H. M. Colquhoun ICI Chemicals and Polymers Ltd. Runcorn, England
D. J. Thompson ICI Specialty Chemicals Wilmington, Delaware
and M.V. Twigg European Vinyls Corporation International Brussels, Belgium
Springer Science+ Business Media, LLC
Library of Congress Catalog1ng-1n-PublIcatIon
Data
C o l q u h o u n , H.M. Carbonylation : direct synthesis of carbonyl compounds / H.M. C o l q u h o u n , D . J . Thompson, and M.V. Twigg. p. cm. Includes bibliographical references and index. 1. Carbonyl compounds. III. Title. QD305.A6C623 1991 547' . 0 3 6 — d c 2 0
I. Thompson, D . J .
II. Twigg, M.V.
91-10817 CIP
This limited facsimile edition has been issued for the purpose of keeping this title available to the scientific community. 10 9 8 7 6 5 4 3 2
This book is to provide general information concerning its subject matter; it is not intended to provide detailed procedural instructions. The reader should consult appropriate sources for details of experimental methods and statutory safety regulations. Any person using information on equipment, methods, or materials given in this book should do so only after seeking the advice of a suitably qualified person. While all reasonable care has been used in compiling this book, the authors and publisher accept no responsibility for the accuracy of the contents, nor for any misuse of the book, including its use as a procedural manual. Many of the topics covered in this book are the subject of patents, and therefore nothing contained herein should be construed as granting a license or permission to use any invention or process that may be protected by a patent. ISBN 978-1-4757-9578-3 DOI 10.1007/978-1-4757-9576-9
ISBN 978-1-4757-9576-9 (eBook)
© Springer Science+Business Media New York 1991 Originally published by Plenum Press, New York in 1991 All rights reserved No part of this book may be reproduced, stored in a retrieval system, or transmitted in any form or by any means, electronic, mechanical, photocopying, microfilming, recording, or otherwise, without written permission from the Publisher
Preface Since the publication of our earlier book on transition metal mediated organic synthesis, * there has been a widespread increase of interest in this topic, and transition metal based methodology has become firmly established in many areas of organic chemistry. The direct, catalytic formation of organic carbonyl compounds using carbon monoxide as the source of the carbonyl group has seen exceptional progress, and this carbonylation chemistry is being used increasingly in research and on a larger scale for fine chemicals production. In view of these developments, there is a need for a modem, practically oriented book dealing with transition metal based carbonylation chemistry. The present monograph should help fulfill this need, since it is intended specifically to foster the adoption of catalytic carbonylation as a general tool in synthetic organic chemistry. It deals exclusively with reactions involving the interco
