Shear bond strength of Biodentine, ProRoot MTA, glass ionomer cement and composite resin on human dentine ex vivo

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HEAD & FACE MEDICINE

RESEARCH

Open Access

Shear bond strength of Biodentine, ProRoot MTA, glass ionomer cement and composite resin on human dentine ex vivo Markus Kaup1, Christoph Heinrich Dammann1, Edgar Schäfer2 and Till Dammaschke1*

Abstract Introduction: The aim of this study was to compare the shear bond strength of Biodentine, ProRoot MTA (MTA), glass ionomer cement (GIC) and composite resin (CR) on dentine. Methods: 120 extracted human third molars were embedded in cold-cured-resin and grinned down to the dentine. For each material 30 specimens were produced in standardised height and width and the materials were applied according to manufacturers´ instructions on the dentine samples. Only in the CR group a self-etching dentine-adhesive was used. In all other groups the dentine was not pre-treated. All specimens were stored at 37.5 °C and 100% humidity for 2d, 7d and 14d. With a testing device the shear bond strength was determined (separation of the specimens from the dentine surface). The statistical evaluation was performed using ANOVA and Tukey-test (p < 0.05). Results: At all observation periods the CR showed the significant highest shear bond strength (p < 0.05). After 2d significant differences in the shear bond strength were detectable between all tested materials, whereby CR had the highest and MTA the lowest values (p < 0.05). After 7d and 14d the shear bond strengths of MTA and Biodentine increased significantly compared to the 2d investigation period (p < 0.05). Biodentine showed a significantly higher shear bond strength than MTA (p < 0.05), while the difference between Biodentine and GIC was not significant (p > 0.05). Conclusions: After 7d Biodentine showed comparable shear bond values than GIC, whereas the shear bond values for MTA were significantly lower even after 14d. The adhesion of Biodentine to dentine surface seams to be superior compared to that of MTA. Keywords: Biodentine, Composite resin, Glass ionomer cement, ProRoot MTA, Shear bond strength

Introduction In the early 1990s the development of mineral trioxide aggregate (MTA) introduced a new class of dental calcium silicate cements (CSCs) based on Portland cement, originally developed as a perforation repair material. Since then it has been widely used for repairpurposes of furcations and root canals, as a root-end filling material, for direct and indirect pulp-capping and the treatment of extern and intern resorptions with high success rates [1-3].

* Correspondence: [email protected] 1 Department of Operative Dentistry, Westphalian Wilhelms-University, Albert-Schweitzer-Campus 1, building W 30, 48149 Münster, Germany Full list of author information is available at the end of the article

Beside a long setting time the major drawbacks of MTA are its relatively low compression and flexural strength, which are lower than those of dentine [4]. These factors are limiting the field of application to low stress-bearing areas [5]. Hence, MTA can not be used e.g. as base, base build-up, core material or as temporary restoration