Structure Elucidation by Modern NMR A Workbook
During the last few years, routine applications of NMR techniques have been further developed. Spectrometers of the latest generation offer new types of experiments, such as spinlock and inverse-detected methods. In this third, revised and expanded editio
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Structure Elucidation by Modern NMR
H. Duddeck, W. Dietrich, G. T6th
Structure Elucidation by Modern NMR A Workbook Third, Revised and Updated Edition
Springer
Prof. Dr. Helmut Duddeck University of Hannover, Institute of Organic Chemistry Schneiderberg 1B, 0-3 0167 Hannover, Germany Dr. Wolfgang Dietrich Ruhr University Bochum, Faculty of Chemistry P.O. Box 102148,0-44780 Bochum, Germany Prof. Dr. Gabor T6th Technical Analytical Research Groupof the Hungarian Academy of Sciences Technical University Budapest, lnstitute for General and Analytical Chemistry Szent Gellért tér 4, H-llll Budapest, Hungary
Die Deutsche Bibliothek - CIP-Einheitsaufnahme Duddeck, Helmut:
Structure elucidation by modern NMR : a workbook / H. Duddeck ; W. Dietrich ; G. T6th. - 3., rev. and updated ed. - Darmstadt : Steinkopff; New York : Springer, 1998 Dt. Ausg. u.d.T.: Duddeck, Helmut: Strukturaufklârung mit moderner NMR-Spcktroskopie Dietrich, Wolfgang: Strukturaufklârung mit moderner NMR-Spcktroskopie Toth, Gabor: Strukturaufkliirung mit modemcr NMR-Spcktroskopic
This work ist subject to copyright. Ali rights are reserved, whether the whole or part of the matcrial is concerned, specifically the rights of translation. reprinting. re-use of illustrations. recitation, broadcasting, reproduction on microfilm or in other ways. and storage in data banks. Duplication of this publication or parts thereof is only permitted under the provisions of the German Copyright Law of Septernber 9. 1965. in its version of June 24. 1985. and a copyright fee must always be paid. Violations full under the prosecution act of the German Copyright Law.
ISBN 978-3-7985-1111-8 ISBN 978-3-642-88310-1 (eBook) DOI 10.1007/978-3-642-88310-1 © 1998 by Springer-Verlag Berlin Heidelberg Originally published by Dr. Dietrich Steinkopff VerJag GmbH & Co. KG, Darmstadt in 1998.
Chemistry Editor: Dr. Maria Magdalene Nabbe - Copy Editing: Dr. Mary K. Gossen Production: Heinz J. Schafer The use of rcgistered narnes, trademarks, etc. in this publication does not imply. even in the absence of a specifie staternent, that such narnes arc exempt l'rom the relevant protective laws and regulations and therefore free for general use.
Foreword In 1988, our first workbook (Strukturaujklärung from the Technical University in Budapest, Hungary, to contribute significantly to this new edition. mit moderner NMR-Spektroskopie, Steinkopff, Darmstadt) appeared in the German language He is among the most prominent NMR specialists based on our experience in organizing seminars in his country and abroad, and has been teaching and workshops on the application of modem one- spectroscopy and its application in organic chemiand two-dimensional NMR methods. Many of the stry for more than 20 years. This book cou1d not have been written in the exercises described in the workbook have been used in these courses and some of them have been present form without the help of a number of shaped to a great extent by the participants. The colleagues; therefore, we gratefully acknowledge response of
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