Structure Elucidation by Modern NMR A Workbook
For several years we have been organizing seminars and workshops on the application of modem one and two-dimensional NMR methods at the faculty of chemistry in the Ruhr-University Bochum, FRG, and elsewhere, addressing researchers and graduate students w
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H. Duddeck, W Dietrich
Structure Elucidation by ModemNMR A Workbook
With a Preface by J. B. Stothers
Prof. Dr. H. Duddeck Dr. W Dietrich FakulHit flir Chemie Ruhr-UniversiUit Bochum Postfach 102148 4630 Bochum, FRG
CIP-Titelaufnahme der Deutschen Bibliothek Duddeck, Helmut: Structure elucidation by modern NMR : a workbook / H. Duddeck ; W. Dietrich. With a pref. by 1. B. Stothers. Darmstadt: SteinkoptT ; New York: Springer, 1989 Dt. Ausg. u. d. T.: Duddeck, Helmut: StrukturaufkJiirung mit moderner NMR-Spektroskopie ISBN-13: 978-3-7985-0787-6 e-ISBN-13: 978-3-642-97781-7 DOl: 10.1007/978-3-642-97781-7
NE: Dietrich, Wolfgang: This work is subject to copyright. All rights are reserved, whether the whole or part of the material is concerned, specifically the rights of translation, reprinting, re-use of illustrations, recitation, broad-casting, reproduction on microfilms or in other ways, and storage in data banks. Duplication ofthis publication or parts thereofis only permitted under the provisions of the German Copyright Law of September 9, 1965, in its version of June 24, 1985, and a copyright fee must always be paid. Violations fall under the prosecution act of the German Copyright Law. Copyright © 1989 by Dr. Dietrich Steinkopff Verlag GmbH & Co. KG, Darmstadt Chemist Editor: Heidrun Sauer - Copy Editing: Marilyn Salmansohn - Production: Heinz 1. Schiifer
The use of registered names, trademarks, etc. in this publication does not imply, even in the absence of a specific statement, that such names are exempt from the relevant protective laws and regulations and therefore free for general use.
Foreword
For several years we have been organizing seminars and workshops on the application of modem oneand two-dimensional NMR methods at the faculty of chemistry in the Ruhr-University Bochum, FRG, and elsewhere, addressing researchers and graduate students who work in the field of organic and natural products chemistry. In 1987, we wrote a workbook (StrukturaufkUirung mit modemer NMR-Spektroskopie, Steinkopff, Darmstadt, FRG, 1988) in German language based on our experience in these courses. Many of the exercises described therein have been used in such courses and some of them have been shaped by the participants to a great extent. The response of readers and discussions with colleagues from many countries encouraged us to produce an English translation in order to make the book accessible to a wider audience. Moreover, the content has been increased from 20 exercise examples in the German, to 23 in the English version. This book could not have been written in the present form without the help of a number of colleagues and, therefore, we acknowledge gratefully the generous supply of samples from and useful discussions with B. Abegaz (Addis Ababa, Ethiopia), U.H. Brinker (Bingham, New York, USA), E. Dagne (Addis Ababa, Ethiopia), M. Gonzalez-Sierra (Rosario, Argentina), J. Harangi (Debrecen, Hungary), SA Khalid (Khartoum, Sudan), A. Levai (Debrecen, Hungary), MA McKervey (Cork, Ireland), M. Michalska (Lodz ,Poland
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