Structure Elucidation by Modern NMR A Workbook
For several years, we have been organizing seminars and workshops on the application of modem one and two-dimensional NMR methods at the faculty of chemistry in the Ruhr-University Bochum, FRG, and elsewhere, addressing researchers and graduate students
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H. Duddeck, W. Dietrich
Structure Elucidation by ModernNMR A Workbook 2nd, revised and enlarged edition With Prefaces by J. B. Stothers and K. Nakanishi
~ SteinkopffVerlag Darmstadt
i
Springer-Verlag New York
Prof. Dr. Helmut Duddeck Dr. Wolfgang Dietrich Fakultat flir Chemie Ruhr-Universitat Bochum Postfach 102148 4630 Bochum, FRG
Die Deutsche Bibliothek - CIP-Einheitsaufnahme Duddeck, Helmut: Structure elucidation by modern NMR : a workbook I H. Duddeck; W. Dietrich. With pref. by J. B. Stothers and K. Nakanishi. - 2., rev. and en!. ed. - Darmstadt: Steinkopff ; New York: Springer, 1992 Dt. Ausg. u.d.T.: Duddeck, Helmut: Strukturaufklarung mit moderner NMR-Spektroskopie ISBN-13: 978-3-7985-0930-6 DOl: 10.1007/978-3-642-97787-9
e-ISBN-13: 978-3-642-97787-9
NE: Dietrich, Wolfgang: This work is subject to copyright. All rights are reserved, whether the whole or part of the material is concerned, specifically the rights of translation, reprinting, re-use of illustrations, recitation, broadcasting, reproduction on microfilms or in other ways, and storage in data banks. Duplication of this publication or parts thereof is only permitted under the provisions of the German Copyright Law of September 9, 1965, in its version of June 24, 1985, and a copyright fee must always be paid. Violations fall under the prosecution act of the German Copyright Law. Copyright © 1992 by Dr. Dietrich SteinkopffVerlag GmbH & Co. KG, Darmstadt Chemistry Editor: Dr. Maria Magdalene Nabbe - Copy Editing: Marilyn Salmansohn, James C. WillisProduction: Heinz J. Schafer
The use of registered names, trademarks, etc. in this publication does not imply, even in the absence of a specific statement, that such names are exempt from the relevant protective laws and regulations and therefore free for general use.
Foreword
For several years, we have been organizing seminars and workshops on the application of modem oneand two-dimensional NMR methods at the faculty of chemistry in the Ruhr-University Bochum, FRG, and elsewhere, addressing researchers and graduate students who work in the field of organic and natural products chemistry. In 1987, we wrote a workbook (StrukturaufkUirung mit modemer NMR-Spektroskopie, Steinkopff, Darmstadt, FRG, 1988) in German language based on our experience in these courses. Many of the exercises described therein have been used in such courses and some of them have been shaped by the participants to a great extent. The response of readers and discussions with colleagues from many countries encouraged us two years later to produce an English translation in order to make the book accessible to a wider audience. Moreover, the content has been increased from 20 exercise examples in the German, to 23 in English version. Now, after the rapid development of basic multipulse NMR methods in the early 1980s, the avantgarde in modem NMR is concentrating on the invention and optimization of advanced techniques, e.g., three-dimensional experiments. For the beginners, however, the situation has not changed markedly since t
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