A new method for single step sonosynthesis and incorporation of ZnO nanoparticles in cotton fabrics for imparting antimi

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ORIGINAL PAPER

A new method for single step sonosynthesis and incorporation of ZnO nanoparticles in cotton fabrics for imparting antimicrobial property Aravind H. Patil1,2 · Pramod S. Patil1,2   · Sushilkumar A. Jadhav2   · Vikramsinh B. More3 · Kailas D. Sonawane3 · Shirishkumar H. Vhanbatte4 · Pradyumna V. Kadole4 Received: 23 June 2020 / Accepted: 12 September 2020 © Institute of Chemistry, Slovak Academy of Sciences 2020

Abstract An efficient and effective sonosynthesis technique for the synthesis and simultaneous incorporation of Zinc oxide nanoparticles (ZnO NPs) on cotton fabrics is developed. The surface plasmon resonace (SPR) of ZnO NPs was studied using UV–visible spectroscopy and the average hydrodynamic diameter of the particles was determined by dynamic light scattring (DLS). The ZnO NPs incorporated cotton fabrics were characterized by X-ray diffraction (XRD), attenuated total reflectance Fourier transform infrared (ATR-FTIR) spectroscopy and Scanning electron microscopy (SEM). The tensile strength, flexural rigidity, air permeability, and water contact angle of the ZnO NPs deposited cotton fabrics were measured and compared with the pristine cotton. The SEM images showed excllent deposition of the NPs on the cotton yarns. Textile engineering characterization revealed that the inherent properties of cotton fabric remain in acceptable limits after deposition of the NPs. The ZnO NPs deposited cotton fabrics exhibited excellent antibacterial activities against Escherichia coli and Staphylococcus aureus bacteria. Graphical abstract

Keywords  Zinc oxide nanoparticles · Sonochemical technique · Cotton · Nanotextile · Antibacterial efficacy Electronic supplementary material  The online version of this article (https​://doi.org/10.1007/s1169​6-020-01358​-0) contains supplementary material, which is available to authorized users. * Pramod S. Patil [email protected]

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School of Nanoscience and Technology, Shivaji University Kolhapur, Vidyanagar, Kolhapur 416004, Maharashtra, India

* Sushilkumar A. Jadhav [email protected]

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Department of Microbiology, Shivaji University Kolhapur, Vidyanagar, Kolhapur 416004, Maharashtra, India

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D.K.T.E. Society’s Textile and Engineering Institute, Ichalkaranji 416115, Maharashtra, India

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Department of Physics, Shivaji University Kolhapur, Vidyanagar, Kolhapur 416004, Maharashtra, India

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Introduction Textile substrates act as a good media for the growth and proliferation of microorganisms, such as virus, bacteria, and fungi at a particular temperature and humidity (Yuan Gao and Cranston 2008; Iyigundogdu et al. 2017). The growth of microorganisms can harm the textile as well as the user (Morais et al. 2016). It leads to the formation of irritating odor, and reduction in the tensile strength of textiles (Morais et al. 2016). To overcome such issues, intensive research is going on to develop antimicrobial nanotextiles by incorporation of nanophased materials in textiles (Harifi and Montazer 2015; Morais et al. 2016; V