Development of a Microwave-Assisted Extraction Method for the Determination of Organochlorine Pesticides in Mussel Tissu
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Development of a Microwave-Assisted Extraction Method for the Determination of Organochlorine Pesticides in Mussel Tissue Emmanouil-Nikolaos Papadakis & Archontoula Kyrgidou & Zisis Vryzas & Euphemia Papadopoulou-Mourkidou
Received: 22 May 2013 / Accepted: 16 October 2013 # Springer Science+Business Media New York 2013
Abstract A method for the multiresidue analysis of 16 organochlorine insecticides in mussel tissue was developed. The method was based on the microwave-assisted extraction of the mussel tissue by the use of acetonitrile followed by the solid phase extraction (SPE) cleanup of the extracts and subsequent analysis by GC/MS in the selected ion monitoring (SIM) mode. Microwave-assisted extraction (MAE) operational parameters (extraction temperature and time, extractant volume) were optimized with respect to extraction efficiency of the target compounds. Recoveries >70 % with percent relative standard deviation (RSD%)
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